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Rabu, 16 Maret 2016

KRUSS Dynamic Foam Analyzer – DFA100

KRUSS Dynamic Foam Analyzer – DFA100


Scientific analysis of liquid foams

Our DFA100 instrument for analyzing foams measures the foamability of liquids and the foam stability based on precise measurements of the foam height. With flexibly deployable modules, it also measures the liquid content of the foam or analyses the foam structure with regard to bubble size and distribution. The DFA100 assists in the optimization of foam-forming products or, in the case of unwanted foam formation, helps with specific foam prevention.

Reproducible, precise and process-related measurements

A particular strength of our DFA100 is the exceptional reproducibility of foam height measurements thanks to an accurately controlled foaming process with electronic gas flow control. The optical sensor measures the quantity of foam produced and the decay characteristic equally precisely and with high resolution, even with very short-lived foams. As a result, the DFA100 is a reliable instrument for analyzing the whole spectrum from slow to very fast decaying foams. Specific measures for avoiding foam can be taken and the quantity and stability of the foam can be optimized with the help of the results obtained.
We have provided options for producing foam by means of bubbles or by stirring, in order to simulate process conditions and to be able to transfer raw data to large-scale situations. As further options, you can also simulate process temperatures up to 90°C or use externally connected gases such as carbon dioxide.

Impressively easy to use

The ease of using the DFA100 when preparing the measurement and when cleaning is of great advantage. The measuring cylinder is simply placed in the instrument using the plug-in unit. The flexible system enables components to be cleaned quickly, and allows one sample to be prepared while another measurement is running. This means more measurements in the same time.
The simple operation of the instrument goes hand-in-hand with the intuitive user guidance of the foam analysis software. The transparent programming of the measurement and the clear data management ensure rapid familiarization and effective use of the DFA100 from day one. After starting, the software controls the whole measurement, including the evaluation. Automatic multiple measurements provide statistical backup of the results.

Tasks and applications

  • Foams for washing and cleaning
  • Firefighting
  • Foams in foodstuffs and body care products
  • Surfactant development
  • Flotation as a method for separating solids
  • Foam-inhibiting and foam-reducing agents (Antifoamers / Defoamers)
  • Foam prevention for paints and varnishes, process and waste water and cooling lubricants

Measuring methods and options

  • Measurement of foamability of liquids and foam decay
  • Determination of total height, foam height and liquid height
  • Foaming by means of bubbles or stirring
  • Investigations of externally produced foams
  • Automatic multiple measurements
  • Foamability parameters, including maximum height, foam capacity and foam density
  • Decay parameters, including start of decay, decay half-life and time-dependent foam heights similar to Ross-Miles
  • Temperature-controlled measurements up to 90°C
  • Foaming with externally connected gases

Technical Data

Maximum measuring height200 mm
Height resolution0.125 mm
Maximum frame rate20 frames per second
Minimum sample volume20 ml
Gas flow when bubbling0.2 to 1.0 L/min (standard)
0.05 to 1.0 L/min (externally connected gas)
Rotational speed when stirringmaximum 8000 rpm
Dimensions245 × 275 × 460 mm (W × D × H)
Weight9 kg

KRUSS Large Surface Analyzer - LSA

KRUSS Large Surface Analyzer - LSA




The robotic system for very fast wetting analyses of big-sized samples

Fully automatic measurements on many positions of large sample areas: Our Large Surface Analyzer – LSA combines a precise positioning robot with our Mobile Surface Analyzer – MSA for measuring surface free energy within a second. The system is especially suitable for quality control of cleaned, pre-treated or coated large surfaces due to its easy handling and programming as well as high measuring speed.

Measurement of surface free energy within a second

The automatically moved MSA, with its ability to take measurements in less than one second, is the fastest mobile instrument on the market for determining surface free energy with two test liquids. It does this by means of a non-contact pressure dosing system that places two drops on the sample, followed by an automatic image analysis of each drop including contact angle measurement and SFE calculation. With our Large Surface Analyzer – LSA, these features are enhanced using the quick and precise positioning of the instrument between measurements.

Powerful positioning robot in different sizes

The Large Surface Analyzer – LSA has one vertical and two horizontal axes and is designed to handle sample sizes of 495 × 565 mm. A second standard model allows operators to position the instrument as desired on an even larger surface of 2900 × 3150 mm. Upon request, customized systems in other sizes are possible.

Tasks and applications

  • Pre-treatment and coating of large components
  • Cleaning and coating of glass surfaces
  • Wetting analyses on printing plates

Measuring methods and options

  • Determining surface free energy with two test liquids
  • Measuring contact angle
  • Position-dependent measurements (mapping)

KRUSS Mobile Surface Analyzer – MSA

KRUSS Mobile Surface Analyzer – MSA



Measuring surface free energy in a second with only one click

Our innovative Mobile Surface Analyzer – MSA measures surface free energy with two liquids, fully automatically and mobile using our new “One-Click SFE” method. The MSA doses two parallel drops with one click, followed by the direct analysis of the contact angles and the derived results of the surface free energy. All steps are automated and happen within a second. The results enable well-founded statements about wettability by aqueous or organic liquids. The MSA supports you in your quality assurance in the pre-treatment and coating of solid materials in an ideal way.

New, innovative dosing unit for parallel analysis with two test liquids

Our innovative, specially developed double dosing system doses two parallel drops within milliseconds, with high volume precision and minimal kinetic energy. This simultaneous dosing of two drops obviates the need to change the test liquid during the material analysis, as is the case with conventional dosing units. The contactless method prevents unwanted touching of the sample with possible contamination or damage.
Cartridges that can easily be refilled outside the instrument make for simple operation of the dosing system. Fully charged, the handy instrument is capable of dosing 1,000 droplets of each liquid.
We have developed an alternative dosing solution which uses conventional disposable syringes for liquids that require extensive cleaning effort such as adhesives, inks or paints. The conversion to this automatic syringe dosing module is done very quickly.

Simple in operation and flexible in use

The MSA is preferably used with a notebook. Due to the USB power connection, its low weight and small footprint the MSA is ideal for the mobile and non-destructive quality control. The instrument analyses samples of any size, such as automobile bodies. It provides reliable values even for vertical, overhead and slightly convex samples.
Our modern, intuitive ADVANCE – Drop Shape software automatically calculates the surface free energy based on proven and meaningful scientific models. For example, information gained about the polarity of the surface provides a reliable indication of the effect of activation by such methods as plasma treatment.
The precise measurement and scientific evaluation are performed with a single button click. Thus, measurement errors due to incorrect operation are virtually ruled out.

Tasks and applications

  • Measurement on large workpieces and finished products such as automobile parts
  • Determination of the wettability of solid materials before coating or bonding
  • Quality assurance of pre-treatment and coating processes
  • Quality assurance of cleaning steps
  • Testing the effectiveness of hydrophobic coatings

Measuring methods and options

Accessories

Technical data

Resolution0.1°
Footprint32 x 84 mm
Weight0.85 kg

KRUSS Drop Shape Analyzer – DSAHT

KRUSS Drop Shape Analyzer – DSAHT




High-temperature measurement of contact angle and surface tension

Our DSAHT specializes in the precise high-temperature measurement of wetting based on contact angle and surface tension. Materials such as metals, glass or ceramics in molten form can be investigated using our DSAHT at actual process and working temperatures. To this end, our high-quality, optical drop shape analysis components work together with first-class high-temperature furnaces which have excellent temperature consistency and homogeneity. The accurate measuring results at temperatures up to 1750 °C contribute to the optimization of processes such as metal smelting, the combustion of biomass and enameling.

High-quality optical solutions for precision measurements

Our high-resolution camera and quality lens together with the zoom option and accurate focusing guarantee outstanding image quality of the molten drop. A special filtering technique filters out the inherent radiance of glowing samples. This ensures a high-contrast contour for the shadow image, thus enabling the drop image to be accurately analyzed by optical means. The intelligent evaluation algorithms in our software also ensure precise results when measuring contact angle and surface tension.

Intelligent furnace design for accurate temperature control

The furnace of our DSAHT has been developed with high temperature accuracy in mind. The long length of the furnace tube guarantees a particularly homogenous temperature distribution in the vicinity of the sample. The long length of the tube also ensures a flat temperature gradient from the hottest point towards the ends, thus avoiding stresses which can affect the material. The precision temperature sensor is set directly into the sample table in order to measure the sample temperature exactly and enable it to be controlled accurately.
The furnace can be opened quickly and easily and the sample easily loaded thanks to intelligently designed flanges and a sliding device. The furnace can remain closed while the sample is aligned. This saves considerable time, as otherwise the furnace would first have to be cooled down in order to correct the sample position after loading the sample.
We provide the optimum instrument for your required target temperature with different versions of our DSAHT with temperatures up to 1200 °C, up to 1500 °C or up to 1750 °C. The furnace tube works flexibly under oxidizing, inert or reducing atmospheres and under vacuum (up to 1000 °C). This enables real conditions for wetting melts in particular processes to be simulated, thus enabling the results to be used for optimizing these processes.

Intelligent software with many analysis options

Our temperature control and drop shape analysis software opens up a variety of measuring options. As well as setting a constant target temperature, accurately controlled temperature ramps can also be programmed. By this means, accurate analyses of smelting and redistribution processes, for example changes to the green body in ceramic production, can be carried out. The software can also record single frames and videos at programmed intervals in order to document changes in the material. Beneath others, this option enables cinder cones to be precisely investigated in accordance with the ASTM D-1857 standard for optimizing process control in combustion reactors.

Tasks and applications

  • Smelting
  • Glass manufacture
  • Enamel coatings
  • Ceramics
  • Metallurgy
  • Optimization of combustion processes

KRUSS Top View Analyzer – TVA100

KRUSS Top View Analyzer – TVA100



Special instrument for measurements in depressions and on concave surfaces

Our Top View Analyzer – TVA100 is the only instrument in the world to use the top-view reflection method for measuring the contact angle of a liquid on a solid from above. The innovative measuring method is particularly suitable for measurements in depressions and on concave surfaces where drops cannot be analyzed using the conventional side view.

High-quality components for precise contact angle

The instrument measures the contact angle of the drop based on the distance of light spots which are reflected at the surface of the drop. The instrument is equipped with a high-quality lens and a high-resolution camera in order to display this distance accurately. The drop, the volume of which is included in the calculation, is dispensed with high precision in order to obtain a reliable value for the contact angle.
Measurements are quickly carried out with several test liquids by changing the dosing tips in a simple way in order to determine the surface free energy of the sample. Prepared measurement templates in the software for the measurement of contact angle and surface free energy save more time when carrying out the measurements and provide easy familiarization.

Flexible use of measuring head for other systems

The measuring head used in the TVA100 is also available as a module for our Drop Shape Analyzers DSA100 and DSA30. When incorporated into these modular systems, it enables a fast changeover between the top-view reflection method and the horizontal method for drop shape analysis by means of a simple conversion.
We would also be pleased to develop a suitable, special gantry solution for your application for moving the TVA100 measuring head accurately to the required measuring position with the help of a robot.

Tasks and applications

  • Measurements in depressions of well plates
  • Measurement between electronic components on populated boards
  • Measurement on concave optical lenses
  • Surface investigations for the interior of tubes and hoses

KRUSS MobileDrop

KRUSS MobileDrop




Flexible contact angle measurement on site for quality assurance

Our MobileDrop has been specially developed for mobile use. The handy instrument determines the wettability and surface free energy of solids based on the contact angle. It carries out precise, non-destructive measurements on samples of any size, and even measures vertically or on the underside of a surface. The simple operation and rapid measurement makes the MobileDrop particularly well-suited to quality assurance and process optimization, for example in the cleaning, pre-treatment and coating of materials.

Measure easily and quickly on the move

The lightweight instrument, weighing just 500 g, contains a complete measuring system with camera, dosing unit and lens. Thanks to its ergonomic shape, the MobileDrop can be easily operated with one hand. Connected only to a notebook for evaluating data, the MobileDrop measures reliably, independently of the electricity supply, and flexibly with regard to location.
We have developed quickly changeable dosing units - for taking more measurements in the same time - for measuring the surface free energy with several liquids.
Our modern, intuitive ADVANCE – Drop Shape software automatically calculates the surface free energy based on proven and meaningful scientific models. For example, information gained about the polarity of the surface provides a reliable indication of the effect of activation by such methods as plasma treatment.

Questions and applications 

  • Measurement on large workpieces and finished products such as automobiles or walls
  • Determination of the wettability of solid materials before coating or bonding
  • Quality assurance of pre-treatment and coating processes
  • Quality assurance of cleaning steps
  • Checking the effectiveness of hydrophobic coatings

Measuring methods and options

Technical data

Measuring range5 to 175°
Resolution0.1°
Footprint25 × 52 mm
Weight0.5 kg

Selasa, 15 Maret 2016

KRUSS Drop Shape Analyzer – DSA30E

KRUSS Drop Shape Analyzer – DSA30E


Comprehensive options for ensuring the quality of wetting and coating processes

The expert version of our DSA30 enables solid and liquid phases in wetting and coating processes to be analyzed with a high degree of automation. The DSA30E measures the contact angle andsurface free energy of solids and the surface tension of liquids reliably and precisely. The instrument is ideal for standardized quality assurance with a high frequency of samples.
Our DSA30E is fitted with three software-controlled axes. These move the sample accurately and quickly to all programmed measuring positions, where dosing and measurement are then carried out fully automatically. Our software-controlled dosing unit with up to four test liquids measures the contact angle in rapid succession and in any sequence. An automatically determined and accurate value of the surface free energy is therefore available after a short measuring period.
Our special dosing feed with accurately adjustable drop volume guarantees particularly precise and highly reproducible measuring conditions. Our DSA30E also enables the advancing and receding angles to be measured. This averages out local inhomogeneities in the sample and enables theroughness of the solid to be assessed.
The measurement runs fully automatically based on programmable measuring sequences which we have already prepared for the main surface analysis tasks.
The measurement of surface tension can be carried out without reconfiguring the instrument, and can even be incorporated into an automatic measuring sequence. Combining the liquid data with those of a solid enables the compatibility of the two phases to be comprehensively characterized. By this means, for example, it is possible to determine the intensity of the adhesion and the long-term stability of a coating.

Features

  • Software-controlled x and y-axis and software-controlled lift table (z-axis)
  • Software-controlled quadruple-dosing unit
  • Zoom lens (6.5-times)
  • Camera with 780 × 580 px resolution
  • Very bright, homgenous LED illumination
  • Software for measuring contact angle, surface free energy of solids and surface tension of liquids

KRUSS Drop Shape Analyzer – DSA100

KRUSS Drop Shape Analyzer – DSA100


The universal, high-quality instrument for analyzing wetting and coating processes

Our Drop Shape Analyzer – DSA100 is our high-quality system solution for almost all tasks in the analysis of wetting and adhesion on solid surfaces. From the basic unit for precise measurement of the contact angle to the fully automatic expert instrument for serial measurement of surface free energy, we have the suitable DSA100 for your special requirements. We exactly match the individual, flexible and reliable components to your surfaces and processes.

Flexible solutions for your tasks

We have developed all components of the DSA100 to provide solution-oriented support in the investigation and optimization of wetting and adhesion behavior. With up to three axes for sample positioning, the sample is moved quickly and reproducibly to the measuring positions. Measurement of the contact angle with up to 8 liquids ensures maximum accuracy when determining the surface free energy. Precisely controlled tempering and humidity chambers help to provide a realistic modeling of the process conditions. Our special sample tables optimize the investigation of wafers and ultrahydrophobic surfaces. High-tech solutions for optical components enable a time-saving, automatic image setup, and measurement of extremely fast wetting processes. They also allow measurements to be made on microscopically small samples.

Quality down to the last detail

The particularly uniform LED illumination and the quality lens ensure high precision when displaying the drop for accurately measuring the contact angle or surface tension. Thanks to the large zoom range, even small drops appear with optimum width in the video image and can therefore be investigated reliably. We have also provided protection for sensitive components and have minimized the troublesome effect of vibration. The high-resolution camera, the lens and the syringes and storage vessels for test liquids are mounted in a robust, enclosed housing.
It is often necessary to adjust the viewing angle before measuring the contact angle. This is achieved particularly quickly and easily with our DSA100. The position of the drop in the image remains unchanged when the viewing angle is adjusted. As a result, the otherwise usual tracking of the sample height is no longer necessary. This innovative optical arrangement also creates space for large samples.

Comprehensive analysis of solids and liquids

Our DSA100 measures the surface tension of liquids using the Pendant Drop method. The results can be used to analyze the relationship between the wetting of the solid and the liquid properties. The results help to provide a scientific picture of the interface contact, which can be used, for example, to optimize the adhesion and long-term stability of coatings. Other solutions for measuring the liquid-liquid interfacial tension, for measurements at high pressures and for surface rheology make the DSA100 a universal instrument for interface research.

Tasks and applications

  • Characterization of surface pre-treatment processes
  • Investigation of the adhesion and stability of bonding and coating processes
  • Investigation of coating substances in accordance with DIN 55660
  • Checking the wettability of plastic, glass, ceramic, wood or metal
  • Quality control for wafers and microelectronics
  • Checking surface cleanliness
  • Elasticity of liquid films
  • Wetting of microscopically small surfaces

Measuring methods and options

  • Contact angle between a liquid and a solid
  • Surface free energy from contact angles of several test liquids using all common models
  • Static contact angleadvancing angle and receding angle
  • Roll-off angle on hydrophobic and superhydrophobic surfaces
  • Measurement of surface tension and liquid-liquid interfacial tension using the Pendant Drop method
  • Temperature-controlled measurements from -30 to 400°C
  • Measurements at controlled humidity
  • Surface rheological measurements (modulus of elasticity E'; modulus of viscosity E'')
  • Wetting measurements on microscopically small surfaces

Accessories (selection)

This list includes a selection of components which are not included in one of the DSA100 versions listed on the right.
  • Tempering chamber for large samples from -10 to 120°C
  • Tempering chamber for rapid temperature changes from -30 to 160°C
  • Tempering chamber for high temperatures up to 400°C
  • High-temperature dosing unit up to 400°C
  • Module for controlling humidity
  • Tilting tables
  • Large instrument frame for large samples
  • Special sample holders, for example for cylindrical samples, films, contact lenses or powders
  • Dosing accessory for Captive Bubble measurements or measurement of the liquid-liquid interfacial tension
  • Dosing units for drops of a few picoliters
  • Module for characterizing the surface rheological properties of liquids

Technical data

Measuring range 
(referred to image analysis)

Contact angle
Surface tension


1-180°
0.01 to 1000 mN/m
Measurement resolution
Contact angle
Surface tension

0.1°
0.01 mN/m
Zoom7 times
Camera resolution
(standard camera)
780 × 580 px
Dimensions
(standard frame)
555 × 375 × 490 mm (W × D × H)
Weightapprox. 35 kg
(depending on configuration)

KRUSS Force Tensiometer – K6

KRUSS Force Tensiometer – K6



The manual tensiometer for clear and reliable basic measurements

Our Force Tensiometer – K6 is a robust and reliable manual instrument for measuring surface tension and interfacial tension using the ring method. As a quality product from our precision mechanical workshop, it produces fast, easy and accurate measurements for surfactant solutions and solvents.
The heart of the instrument is a torsion wire which is connected to a measuring ring. To make the measurement, the ring is immersed in the sample and slowly withdrawn by lowering the liquid. As the ring is withdrawn, the surface tension causes the wire to twist and its defection is indicated on a scale which is calibrated for the surface tension. The result of the measurement is indicated accurately to 1 mN/m.
The horizontal alignment of the instrument, which is necessary to achieve precision measurements, is provided by a special platform with leveling facility. Our K6 has a large measuring range of 1 to 90 mN/m. It therefore measures high surface tensions, such as that of water, and low surface tensions, such as that of hexane and other solvents, equally reliably.
As well as simple investigations of liquid and liquid-liquid interfaces, our K6 is also suitable for training purposes in schools and universities for demonstrating the action of the surface tension force in a comprehensible manner.